技術(shù)文章
Technical articles海關(guān)總署公告 2019年第142號、第166號和第222號發(fā)布的出入境檢驗檢疫行業(yè)標準將分別于2020年3月1日、5月1日和7月1日實施,濟南賽暢科學儀器有限公司整理了公告中涉及到液相、氣相檢測方法的標準制作了耗材速查表,供各位分析人員快速查詢。
實施日期 | 標準號 | 標準名稱 | 前處理耗材名稱(規(guī)格) | 前處理耗材貨號 | 分析耗材名稱(規(guī)格) | 所需色譜柱貨號 |
2020/3/1 | SN/T 5111-2019 | 進出口食用動物、飼料吡喹酮藥物殘留測定 | Cleanert®PEP(500mg/6mL) | PE5006 | Luna® C18(2) (5μm,150mm*2.0mm) | 00F-4252-B0 |
液相色譜-質(zhì)譜/質(zhì)譜法 | ||||||
2020/3/1 | SN/T 5112-2019 | 進出口食用動物、飼料丙二醇含量測定 | Cleanert MAS-Q 2mL凈化管( PSA 50mg;C18 100mg;MgSO4(無水) 100mg) | MS-9PA0205 | Zebron® ZB-WAX,30m*0.25mm*0.25μm | 7HK-G007-11 |
氣相色譜法和氣相色譜-質(zhì)譜法 | ||||||
2020/3/1 | SN/T 5113-2019 | 進出口食用動物、飼料中呋喃測定 | — | — | 硝基呋喃代謝物:Luna Omega C18 (1.6μm,100mm*2.1mm) | 00D-4742-AN |
液相色譜-質(zhì)譜/質(zhì)譜法和液相色譜法 | 呋喃類原藥:Luna Omega C18 (1.6μm,50mm*2.1mm) | 00B-4742-AN | ||||
2020/3/1 | SN/T 5114-2019 | 進出口食用動物、飼料氟苯尼考(氟甲砜霉素)測定 | — | — | Luna Omega C18 (1.6 μm,100mm*2.1mm) | 00D-4742-AN |
液相色譜-質(zhì)譜/質(zhì)譜法 | ||||||
2020/3/1 | SN/T 5115-2019 | 進出口食用動物、飼料中卡巴氧測定 | Cleanert PAX(500mg/3mL) | AX5003 | Kinetex® PS C18 (2.6 μm,100mm*2.1mm) | 00D-4780-AN |
液相色譜-質(zhì)譜/質(zhì)譜法 | Cleanert C18(10g/瓶) | S180010 | ||||
2020/3/1 | SN/T 5116-2019 | 進出口食用動物、飼料孔雀石綠、結(jié)晶紫測定 | Cleanert Alumina N(1g/3mL) | AL0003-N | Kinetex Polar C18 (2.6 μm,50mm*4.6mm) | 00B-4759-E0 |
液相色譜-質(zhì)譜/質(zhì)譜法 | Cleanert PCX(60mg/3mL) | CX0603 | ||||
2020/3/1 | SN/T 5117-2019 | 進出口食用動物、飼料 鏈霉素類(鏈霉素、二氫鏈霉素)藥物殘留測定 | Cleanert PEP (60mg/3mL) | PE0603 | — | — |
液相色譜-質(zhì)譜/質(zhì)譜法 | ||||||
2020/3/1 | SN/T 5118-2019 | 進出口食用動物、飼料中三聚氰胺殘留測定 | Cleanert PCX(60mg/3mL) | CX0603 | Kinetex HILIC (2.6 μm,100mm*2.1mm) | 00D-4474-AN |
液相色譜-質(zhì)譜/質(zhì)譜法 | ||||||
2020/3/1 | SN/T 5119-2019 | 進出口食用動物中新霉素藥物殘留測定 | Cleanert C18(500mg/6mL) | S185006 | — | — |
酶聯(lián)免疫吸附法和液相色譜-質(zhì)譜/質(zhì)譜法 | ||||||
2020/3/1 | SN/T 5120-2019 | 進出口食用動物、飼料中亞硝酸鹽測定 | Cleanert IC-ODS 1cc | IC-1810 | — | — |
比色法和離子色譜法 | Cleanert IC-Ag 1cc | IC-Ag10 | ||||
2020/3/1 | SN/T 5121-2019 | 進出口食用動物、飼料中伊維菌素殘留測定 | — | — | Kinetex C18 (2.6 μm,100mm*4.6mm) | 00D-4462-E0 |
液相色譜-質(zhì)譜/質(zhì)譜法 | ||||||
2020/5/1 | SN/T 0491-2019 | 出口植物源食品中苯氟磺胺 | Cleanert Silica(500mg/6mL) | SI5006 | Zebron ZB-1701 ,30m*0.25mm*0.25μm | 7HK-G006-11 |
殘留量檢測方法 | ZB-5,30m*0.25mm*0.25μm | 7HK-G002-11 | ||||
2020/5/1 | SN/T 1017.6-2019 | 出口糧谷中葉枯酞殘留量檢測方法 | Cleanert C18(60mg/3mL) | S180603 | Luna Omega C18 (1.6 μm,50mm*2.1mm) | 00B-4742-AN |
2020/5/1 | SN/T 1626-2019 | 出口肉及肉制品中甲硝唑、替硝唑、奧硝唑、洛硝噠唑、二甲硝咪唑、塞克硝唑殘留量測定方法 | Cleanert SCX(60mg/3mL) | SC0603 | Luna Omega PS C18 (1.6 μm,100mm*2.1mm) | 00D-4752-AN |
液相色譜-質(zhì)譜/質(zhì)譜法 | ||||||
2020/5/1 | SN/T 1873-2019 | 出口食品中硫丹殘留量的檢測方法 | Cleanert Florisil(1g/6mL) | FS0006 | Zebron ZB-1701,30m*0.25mm*0.25μm | 7HK-G006-11 |
Zebron ZB-5ms,30m*0.25mm*0.25μm | 7HK-G010-11 | |||||
2020/5/1 | SN/T 1979-2019 | 出口動物源食品中吡喹酮殘留量的測定 | Cleanert Alumina B(1g/6mL) | AL0006-B | Kinetex C18 (5μm,150mm*2.1mm) | 00F-4601-AN |
液相色譜-質(zhì)譜/質(zhì)譜法 | ||||||
2020/5/1 | SN/T 2012-2019 | 出口食醋中苯甲酸、山梨酸的檢測方法 | — | — | Luna C18(2) (5μm,150mm*4.6mm) | 00F-4252-E0 |
液相色譜及液相色譜-質(zhì)譜/質(zhì)譜法 | ||||||
2020/5/1 | SN/T 5140-2019 | 出口動物源食品中磺胺類藥物殘留量的測定 | Cleanert PCX(150mg/6mL) | CX1506 | 第二法:Luna C18(2) (3μm,100mm*4.6mm) | 00D-4251-E0 |
Cleanert C18(200mg/3mL) | S182003 | |||||
2020/5/1 | SN/T 5142-2019 | 進出口動物源性食品中粘菌素殘留量的測定 | Cleanert PCX(60mg/3mL) | CX0603 | Luna Omega Polar C18 (3μm,150mm*2.1mm) | 00F-4760-AN |
液相色譜-串聯(lián)質(zhì)譜法 | ||||||
2020/5/1 | SN/T 5143-2019 | 出口小麥粉及其制品中氨基脲的測定 | Cleanert PEP (60mg/3mL) | PE0603 | Kinetex EVO C18 (1.7 μm,50mm*2.1mm) | 00B-4726-AN |
液相色譜-質(zhì)譜/質(zhì)譜法 | ||||||
2020/5/1 | SN/T 5146-2019 | 出口食品中左旋肉堿的測定 | Cleanert PCX(60mg/3mL) | CX0603 | —— | —— |
高效液相色譜和液相色譜-質(zhì)譜/質(zhì)譜法 | ||||||
2020/5/1 | SN/T 5147-2019 | 出口乳制品中肌醇的測定 | — | — | Luna Omega Polar C18 (3μm,100mm*3.0mm) | 00D-4760-Y0 |
液相色譜-質(zhì)譜/質(zhì)譜法 | ||||||
2020/5/1 | SN/T 5148-2019 | 出口動物源食品中可樂定和賽庚啶殘留量的測定 | Cleanert PCX(60mg/3mL) | CX0603 | Luna Omega Polar C18 (1.6μm,100mm*2.1mm) | 00D-4748-AN |
液相色譜-質(zhì)譜/質(zhì)譜法 | ||||||
2020/5/1 | SN/T 5149-2019 | 出口動物源食品中卡麥角林殘留量的測定 | Cleanert Alumina N(1g/3mL) | AL0003-N | Kinetex EVO C18 (1.7μm,150mm*2.1mm) | 00F-4726-AN |
液相色譜-質(zhì)譜/質(zhì)譜法 | ||||||
2020/5/1 | SN/T 5151-2019 | 防曬化妝品中7種二苯酮類物質(zhì)的測定 | — | — | —— | —— |
高效液相色譜法 | ||||||
2020/5/1 | SN/T 5155-2019 | 食品接觸材料檢測方法 高分子材料 食品模擬物中巴豆酸含量的測定 | — | — | Luna Omega Polar C18 (5μm,150mm*2.1mm) | 00F-4754-AN |
高效液相色譜法 | ||||||
2020/5/1 | SN/T 5167-2019 | 出口動物源食品中氫氯噻嗪等10種利尿劑殘留量的測定 | Cleanert MAS-Q 2mL凈化管(MgSO4(無水) 150mg;PSA 50mg;C18 50mg ;PC 7.5mg) | MS-9PP0206 | Luna Omega Polar C18 (3μm,150mm*2.1mm) | 00F-4760-AN |
液相色譜-質(zhì)譜/質(zhì)譜法 | ||||||
2020/5/1 | SN/T 5168-2019 | 出口動物源食品中羥甲烯龍的測定 | — | — | Luna Omega Polar C18 (3μm,100mm*3.0mm) | 00D-4760-Y0 |
液相色譜-質(zhì)譜/質(zhì)譜法 | ||||||
2020/5/1 | SN/T 5169-2019 | 出口動物源食品中美替諾龍的測定 | Cleanert PEP PLUS (200mg/6mL) | PE2006X | Luna Omega Polar C18 (3μm,50mm*2.1mm) | 00B-4760-AN |
液相色譜-質(zhì)譜/質(zhì)譜法 | Cleanert MAS-Q 15mL凈化管(PSA 100mg;C18 40mg; MgSO4(無水)600mg) | MS-9PA1220 | ||||
2020/5/1 | SN/T 5170-2019 | 出口動物源食品中腎上腺素和去甲腎上腺素的測定 | Cleanert PWCX(150mg/6mL) | CX0603 | — | — |
2020/5/1 | SN/T 5171-2019 | 出口植物源性食品中去甲烏藥堿的測定 | Cleanert MAS-Q 2mL凈化管(MgSO4(無水) 150mg;PSA 50mg;C18 50mg ;PC 7.5mg) | MS-9PP0206 | Luna Omega Polar C18 (3μm,100mm*3.0mm) | 00D-4760-Y0 |
液相色譜 - 質(zhì)譜 / 質(zhì)譜法 | ||||||
2020/7/1 | SN/T 5222-2019 | 蜂蜜中20種全氟烷基化合物的測定 | Cleanert MAS-Q 提取包(MgSO4(無水)4g ;NaCl 1g) | MS-MG5055-1 | — | — |
液相色譜-串聯(lián)質(zhì)譜法 | Cleanert C18(10g/瓶) | S180010 | ||||
Cleanert PSA(10g/瓶) | PA0010 | |||||
2020/7/1 | SN/T 5221-2019 | 出口植物源食品中氯蟲苯甲酰胺殘留量的測定 | Cleanert NH2(1g/6mL) | NH0006 | Kinetex C18 (2.6μm,50mm*2.1mm) | 00B-4462-AN |
2020/7/1 | SN/T 5220-2019 | 出口食品中3-氯丙醇酯及縮水甘油酯的測定 | — | — | Zebron ZB-5ms,30m*0.25mm*0.25μm | 7HK-G010-11 |
氣相色譜-質(zhì)譜法 | ||||||
2020/7/1 | SN/T 5219-2019 | 出口食品中氨氯吡啶酸、氯氨吡啶酸殘留量的測定 | Cleanert MAS-Q 提取包(MgSO4(無水)4g ;NaCl1g) | MS-MG5055-1 | — | — |
液相色譜-質(zhì)譜/質(zhì)譜法 | Cleanert C18(10g/瓶) | S180010 | ||||
2020/7/1 | SN/T 5218-2019 | 出口食品中乙酰蓖麻酸酯含量的測定 | — | — | Zebron ZB-5,30m*0.25mm*0.25μm | 7HK-G002-11 |
Zebron ZB-5ms,30m*0.25mm*0.25μm | 7HK-G010-11 | |||||
2020/7/1 | SN/T 5217-2019 | 出口食品中溴化植物油含量的測定 | Cleanert IC-H 1cc | IC-H10 | — | — |
Cleanert C18(250mg/6mL) | S182506 | |||||
2020/7/1 | SN/T 3847-2019 | 出口食品中苯二氮卓類藥物殘留量的測定 | Cleanert PCX(60mg/3mL) | CX0603 | — | — |
液相色譜-質(zhì)譜/質(zhì)譜法 | ||||||
2020/7/1 | SN/T 2574-2019 | 出口蜂王漿中雙甲脒及其代謝產(chǎn)物殘留量的測定 | Cleanert Alumina N(1g/3mL) | AL0003-N | — | — |
液相色譜-質(zhì)譜/質(zhì)譜法 | ||||||
2020/7/1 | SN/T 1594-2019 | 出口茶葉及代用茶中噻嗪酮殘留量的測定 | Cleanert Florisil(1g/6mL) | FS0006 | Zebron ZB-50,30m*0.25mm*0.25μm | 7HK-G004-11 |
Cleanert Florisil(5g/25mL) | FS500025 | |||||
2020/7/1 | SN/T 1071.1-2019 | 出口糧谷中環(huán)庚草醚殘留量的測定 | Cleanert Florisil(1g/6mL) | FS0006 | Zebron ZB-5ms,30m*0.25mm*0.25μm | 7HK-G010-11 |
2020/7/1 | SN/T 0693-2019 | 出口植物源性食品中烯蟲酯殘留量的測定 | Cleanert Alumina N(1g/6mL) | AL0006-N | Zebron ZB-5ms,30m*0.25mm*0.25μm | 7HK-G010-11 |
Cleanert PestiCarb(250mg/6mL) | PC2506 | |||||
Cleanert TPT(2g/10mL) | TPT200010 | |||||
2020/7/1 | SN/T 0654-2019 | 出口水果中克菌丹殘留量的檢測 | Cleanert PestiCarb(10g/瓶) | PC0010 | Zebron ZB-5ms,30m*0.25mm*0.25μm | 7HK-G010-11 |
氣相色譜法和氣相色譜-質(zhì)譜/質(zhì)譜法 | Cleanert C18(10g/瓶) | S180010 | Zebron ZB-5,30m*0.32mm*0.25μm | 7HM-G002-11 | ||
Cleanert PSA(10g/瓶) | PA0010 | |||||
2020/7/1 | SN/T 0337-2019 | 出口植物源性食品中克bai威及其代謝物殘留量的測定 | Cleanert PestiCarb(10g/瓶) | PC0010 | — | — |
液相色譜-質(zhì)譜/質(zhì)譜法 | Cleanert C18(10g/瓶) | S180010 | ||||
Cleanert PSA(10g/瓶) | PA0010 |